I-YY-06 Soxhlet Extractor

Incazelo emfushane:

Isingeniso Sezisetshenziswa:

Ngokusekelwe kumgomo we-Soxhlet extraction, indlela ye-gravimetric yamukelwa ukuze kunqunywe okuqukethwe kwamafutha okusanhlamvu, okusanhlamvu nokudla. Ukuthobelana ne-GB 5009.6-2016 "Izinga Likazwelonke Lokuphepha Kokudla - Ukunqunywa Kwamafutha Ekudleni"; I-GB/T 6433-2006 “Ukunqunywa Kwamafutha Angahluziwe Ekuphakeleni” SN/T 0800.2-1999 “Izindlela Zokuhlola Zamafutha Angahluziwe Wezinhlamvu Nokuphakelayo Okungenisiwe Nokuthekelisa”

Umkhiqizo uklanywe ngokusebenza okuzenzakalelayo kokuchofoza okukodwa ngokugcwele, okubandakanya ukusebenza okulula, ukusebenza okuzinzile nokunemba okuphezulu. Inikeza izindlela eziningi zokukhipha okuzenzakalelayo ezifana ne-Soxhlet extraction, i-hot extraction, i-Soxhlet hot extraction, ukugeleza okuqhubekayo kanye nokukhishwa okujwayelekile okushisayo.

Thumela i-imeyili kithi

Imininingwane Yomkhiqizo

Omaka bomkhiqizo

Izici zesisetshenziswa:

1) Ukuchofoza okukodwa ukuqedela okuzenzakalelayo: yonke inqubo kusukela ekucindezelweni kwenkomishi ye-solvent, ukuphakamisa ubhasikidi wesampula (ukwehlisa) nokufudumeza, ukucwiliswa, ukukhipha, i-reflux, ukubuyisela i-solvent, ukuvulwa nokuvala i-valve.

I-2) Ukucwiliswa kwezinga lokushisa kwegumbi, ukucwiliswa okushisayo, ukukhipha okushisayo, ukukhipha okuqhubekayo, ukukhishwa ngezikhathi ezithile, nokubuyiselwa kwe-solvent kungakhethwa ngokukhululekile futhi kuhlanganiswe.

I-3) I-valve ye-solenoid ingavulwa futhi ivalwe ngezindlela eziningi, njengokusebenza kwephuzu, ukuvula nokuvala okunesikhathi, nokuvula nokuvala ngesandla.

4) Ukuphathwa kwefomula ehlanganisiwe kungagcina izinhlelo zefomula yokuhlaziya engu-99 ehlukene.

I-5) Uhlelo oluzenzakalelayo lokuphakamisa nokucindezela lufaka izinga eliphezulu lokuzenzekelayo, ukwethembeka kanye nokulula.

6) Isikrini sokuthinta sombala esingu-7 intshi sinomklamo osebenziseka kalula, okulula futhi okulula ukuwufunda.

7) Ukuhlela uhlelo olususelwe kumenyu kuyaqondakala, kulula ukusebenza, futhi kungafakwa izikhathi eziningi.

8) Kufika kumasegimenti wohlelo angama-40, amazinga okushisa amaningi, ukucwiliswa kwama-multilevel noma ama-cyclic, ukukhishwa nokushisa.

I-9) Yamukela ibhulokhi yokushisa yokugeza yensimbi ebalulekile, enebanga lokushisa elibanzi kanye nokunemba kokulawula izinga lokushisa eliphezulu.

I-10) Umsebenzi wokuphakamisa okuzenzakalelayo womphathi wenkomishi yephepha lesihlungi uqinisekisa ukuthi isampula icwiliswa ngesikhathi esisodwa ku-solvent ye-organic, okusiza ukuthuthukisa ukuhambisana kwemiphumela yokulinganisa isampula.

I-11) Izingxenye ezenziwe ngezifiso zifanele ukusetshenziswa kwezinyibilikisi zemvelo ezahlukahlukene, kufaka phakathi i-petroleum ether, i-diethyl ether, i-alcohol, okulingiswayo nezinye izinyibilikisi eziphilayo.

12) I-alamu yokuvuza kwe-petroleum ether: Lapho indawo yokusebenza iba yingozi ngenxa yokuvuza kwe-petroleum ether, isistimu ye-alamu iyasebenza futhi imise ukushisisa.

13) Izinhlobo ezimbili zezinkomishi ezincibilikayo, eyodwa eyenziwe nge-aluminium alloy enye ngengilazi, inikezwa abasebenzisi ukuthi bakhethe kuzo.

Izinkomba zobuchwepheshe:

1) Ibanga lokulinganisa: 0.1% -100%

2) Ibanga lokulawula izinga lokushisa: RT+5℃-300℃

3) Ukunemba kokulawula izinga lokushisa: ±1℃

4) Inani lamasampula azokalwa: 6 ngesikhathi

5) Linganisa isisindo sesampula: 0.5g kuya ku-15g

6) Ivolumu yenkomishi ye-solvent: 150mL

7) Izinga lokubuyisela i-solvent: ≥85%

8) Isikrini sokulawula: 7 amayintshi

9) Ipulaki ye-solvent reflux: Ukuvula nokuvala okuzenzakalelayo kwe-Electromagnetic

I-10) Uhlelo lokuphakamisa i-Extractor: Ukuphakamisa okuzenzakalelayo