Indwangu encibilikisiwe inezici zosayizi omncane we-pore, i-porosity ephezulu kanye nokusebenza kahle kokuhlunga, futhi iyisisekelo sokukhiqizwa kwemaski. Leli thuluzi libhekisela ku-GB/T 30923-2014 plastic Polypropylene (PP) Special Material Encibilikisiwe, elungele i-polypropylene njengento eluhlaza eyinhloko, ene-di-tert-butyl peroxide (DTBP) njenge-ejenti yokunciphisa, i-polypropylene encibilikisiwe impahla ekhethekile.
Isampula liyancibilika noma livuvukele ku-toluene solvent equkethe inani elaziwayo le-n-hexane njengezinga langaphakathi. Inani elifanelekile lesixazululo lamuncwa i-microsampler futhi lafakwa ngokuqondile ku-chromatograph yegesi. Ngaphansi kwezimo ezithile, ukuhlaziywa kwe-chromatographic yegesi kwenziwa. Izinsalela ze-DTBP zinqunywe indlela yangaphakathi evamile.
1) I-chromatograph yegesi, i-Capillary column inlet, umtshina we-FID,
2) Hlaziya ibhalansi
3) Ikholomu ye-Capillary: AT.624 30m*0.32mm*1.8μm,
4) Isoftware yeChromatographic workstation,
5) I-N-hexane, i-chromatographic ehlanzekile;
6) I-Di-tert-butyl peroxide, ehlanzekile ngokuhlaziya;
7) I-Toluene, ihlanzekile yokuhlaziya.
I-GC-7890 Gas chromatograph isebenzisa isistimu yokulawula ikhompuyutha encane kanye nesibonisi sesikrini esikhulu sesiShayina, ukubukeka kuhle kakhulu futhi kubushelelezi. Okhiye abasanda kuklanywa bekhibhodi balula futhi bayashesha, futhi amasekhethi ayizingxenye ezingenisiwe, ngakho ukusebenza kwezinsimbi kuzinzile futhi kuthembekile.
Ⅰ. Ukuhlanganiswa kwesekethe ephezulu, ukunemba okuphezulu, imisebenzi eminingi
1. Ukusebenza kokhiye we-microcomputer yonke, 5.7 intshi (320*240) isibonisi esikhulu se-LCD ngesiShayina nesiNgisi, isibonisi sesiShayina nesiNgisi singashintshwa ngokukhululekile, ukuze kuhlangatshezwane nezidingo zamaqembu ahlukene abantu, inkhulumomphendvulwano yomshini womuntu, kulula ukuyisebenzisa .
2.I-Microcomputer yokulawula i-hydrogen flame detector ukuze kuzuzwe umsebenzi wokuthungela okuzenzakalelayo, uhlakaniphe kakhulu. Isekethe entsha yedijithali ehlanganisiwe yedijithali, ukunemba kokulawula okuphezulu, ukusebenza okuzinzile nokuthembekile, kufika ku-0.01℃ ukunemba kokulawula izinga lokushisa.
3.Umsebenzi wokuvikela igesi, vikela ikholomu kanye nechibi le-conductivity eshisayo, umtshina wokubamba ama-electron.
Inomsebenzi wokuzixilonga ekuqaliseni, okwenza abasebenzisi bazi ngokushesha imbangela kanye nesimo sokuhluleka kwensimbi, umsebenzi wesitophuwashi (isilinganiso sokugeleza esilula), ukugcinwa kokwehluleka kwamandla kanye nomsebenzi wokuvikela, umsebenzi wokuphazamisa ukuguqulwa kwamandla, ukuxhumana kwedatha yenethiwekhi. kanye nomsebenzi wokulawula kude. Umsebenzi wokuvikela izinga lokushisa elingaphezulu uqinisekisiwe
Ithuluzi alilimele futhi linesistimu yememori yedatha engadingi ukusetha kabusha konke.
Ⅱ.Idizayini eyingqayizivele yesistimu yomjovo, ingaba umkhawulo wokutholwa ophansi
1. Umklamo wembobo womjovo oyingqayizivele wokuxazulula ukucwaswa komjovo; Umsebenzi wesinxephezelo sekholomu ekabili awuxazululi kuphela ukukhukhuleka komugqa wesisekelo okubangelwa izinga lokushisa elihleliwe, kodwa futhi ususa umthelela womsindo ongemuva ukuze uthole umkhawulo wokutholwa ophansi.
2.Ngekholomu egcwele phama, uhlelo lomjovo we-capillary shunt/non-shunt (nomsebenzi wokuhlanza i-diaphragm)
3.Optional othomathikhi/manual igesi injector six-way, headspace injector, thermal resolution injector, methane converter, othomathikhi injector.
Ⅲ、Izinga lokushisa elihleliwe, ukulawulwa kwezinga lokushisa kwesithando somlilo okunembile, ukuzinza okusheshayo
1.Izinga lokushisa elilinganayo lama-oda ayisishiyagalombili lihleliwe, ngemva komnyango kusetshenziswa idizayini yokushintshanisa yesithombe kagesi, enokwethenjelwa futhi ihlala isikhathi eside, ihlakaniphile ngemva kwevolumu yomoya eguquguqukayo yesistimu yomnyango, finyeza uhlelo ngemva kokukhuphuka/ukwehla kwesikhathi sebhalansi esizinzile sesistimu yomtshina, qaphela ngempela ukusebenza okuseduze kwezinga lokushisa legumbi, ukunemba kokulawula izinga lokushisa kuka-±0.01℃, kuhlangabezana nezidingo zohlaziyo olubanzi.
2.Ivolumu enkulu yebhokisi lekholomu, uhlelo lomnyango wangemuva ohlakaniphile ongenasinyathelo ivolumu yomoya ongena naphuma, finyeza uhlelo ngemva kokuphakamisa/ukupholisa uhlelo lomtshina oluzinzile lwebhalansi; Isistimu yesithando somlilo: izinga lokushisa elizungezile +5 ℃ ~ 420 ℃.
3.I-insulation effect ingcono: ibhokisi lekholomu, ukuhwamuka, ukutholwa ngamadigri angu-300, ibhokisi langaphandle kanye nekhava yangaphezulu kungaphansi kwama-degree angu-40, kuthuthukisa izinga lokuhlola, ukuze kuqinisekiswe ukuphepha komsebenzisi.
4.Idizayini eyingqayizivele yegumbi lokuhwamuka, umthamo omncane ofile; Ukushintshwa kwezinsiza: iphedi lomjovo, i-liner, i-polarizer, umqoqi, umlomo wombhobho ungashintshwa ngesandla esisodwa; Ukushintsha umzimba oyinhloko: ikholomu yokugcwalisa, isampula ye-capillary kanye nomtshina kungasuswa ngokuphelele ngesikrufu kuphela, ukusinakekela kalula.
Ukuzwela okuphezulu, umtshina wokuzinza okuphezulu, ukuhlangabezana nezidingo zezinhlelo ezahlukene
Umtshina we-Hydrogen flame ionization (FID), umtshina we-thermal conductivity cell (TCD), umtshina wokubamba ama-electron (ECD),
Umtshina we-Flame Photometric (FPD), umtshina weNitrogen kanye nePhosphorus (NPD)
Zonke izinhlobo zamadetectors zingalawulwa ngokuzimela izinga lokushisa, umtshina we-hydrogen flame kulula ukuwuhlakaza nokuwufaka, kulula ukuwuhlanza noma ukuwushintsha umbhobho.
Imbobo yomjovo
Izinhlobonhlobo zezimbobo zomjovo ezitholakalayo: umjovo wekholomu ogcwele, umjovo we-shunt/non-shunt capillary
Ibhokisi lokushisa lekholomu
Ibanga lokushisa: izinga lokushisa legumbi +5~420℃
Ukulungiselelwa kwezinga lokushisa: 1 degree; Izinga lokushisa elihleliwe lokunyuka okungu-0.1 degree
Izinga lokushisa eliphakeme kakhulu: 40 degrees/min
Izinga lokushisa elizinzile: 0.01 degree lapho izinga lokushisa le-ambient lishintsha idigri engu-1
Izinga lokushisa elihleliwe: izinga lokushisa le-oda elingu-8 elihleliwe lingashintshwa
Umtshina we-Hydrogen flame ionization (FID)
Izinga lokushisa lokusebenza: 400 ℃
Umkhawulo wokutholwa: ≤5×10-12g/s (n-hexadecane)
I-Drift: 5 x 10-13 a / 30 min noma ngaphansi
Umsindo: 2 x noma ngaphansi 10 kuya ku-13 a
Ibanga lomugqa onamandla: ≥107
Usayizi: 465 * 460 * 550mm, isisindo: 40kg,
Amandla okokufaka: AC220V 50HZ amandla aphezulu 2500W
Imboni yamakhemikhali, isibhedlela, i-petroleum, i-winery, ukuhlolwa kwemvelo, ukuhlanzeka kokudla, inhlabathi, izinsalela zezibulala-zinambuzane, ukwenziwa kwamaphepha, amandla kagesi, izimayini, ukuhlolwa kwempahla, njll.
Ithebula lokulungiselela ithuluzi lokuhlola i-ethylene oxide lamathuluzi ezokwelapha:
Inombolo | Igama | Imininingwane | inombolo ye |
1 | I-chromatograph yegesi | Umsingathi we-GC-7890 (SPL+FID) | 1 |
2 | Ijeneretha yomoya | 2L | 1 |
3 | Ijeneretha ye-hydrogen | 300ml | 1 |
4 | Amasilinda e-nitrogen | Ukuhlanzeka: 99.999% Isilinda + i-valve yokunciphisa ingcindezi (ithengwe endaweni) | 1 |
5 | Ikholomu ezinikezele | Ikholomu ye-capillary | 1 |
6 | Indawo yokusebenza | N2000 | 1 |
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